Matches in SemOpenAlex for { <https://semopenalex.org/work/W2017847493> ?p ?o ?g. }
Showing items 1 to 93 of
93
with 100 items per page.
- W2017847493 endingPage "2384" @default.
- W2017847493 startingPage "2379" @default.
- W2017847493 abstract "Iminophosphocins 8a–8e and 9a–9e were synthesized in four-step reactions via Staudinger reaction. 3-(Bromomethyl)-1,2,3,4,5-pentahydro-3λ5-naphtho[1,8-f,g][1,5,3]diazaphosphocin-3-one (3) was prepared by reacting tris(bromomethyl)phosphineoxide (1) with 1,8-diaminonaphthalene (2) in the presence of triethylamine (TEA) in dry tetrahydrofuran (THF), and treated with L-valine methyl ester (4) and bis(2-chloroethyl)amine (5) in the presence of TEA in dry THF to get 3-methyl-2-[(3-oxo-1,2,3,4,5-pentahydro-3λ5-naphtho[1,8-f,g][1,5,3]diazaphosphocin-3-yl)methylamino]butanoate (6) and 3-[di(2-chloroethyl)aminomethyl]-1,2,3,4,5-pentahydro-3λ5- naphtho[1,8-f,g][1,5,3]diazaphosphocin-3-one (7). The compounds 6 and 7 were treated with trichlorosilane (SiCl3H) in dry tetrahydrofuran (THF) to form the trivalent P(III) intermediates 8 and 9, which were further treated with various alkyl azides in dry THF in 55–60°C to afford the title compounds 8a–8e and 9a–9e. Their structures were established by multi-nuclear NMR and mass spectra. All the newly synthesized compounds were found to possess moderate anti-microbial activity." @default.
- W2017847493 created "2016-06-24" @default.
- W2017847493 creator A5025989570 @default.
- W2017847493 creator A5033848839 @default.
- W2017847493 creator A5038336511 @default.
- W2017847493 creator A5044933041 @default.
- W2017847493 creator A5073284317 @default.
- W2017847493 date "2009-12-01" @default.
- W2017847493 modified "2023-10-09" @default.
- W2017847493 title "Synthesis and Antimicrobial Activity of Novel Iminophosphocin Derivatives" @default.
- W2017847493 cites W1530028876 @default.
- W2017847493 cites W1972712571 @default.
- W2017847493 cites W2066129213 @default.
- W2017847493 cites W2071719043 @default.
- W2017847493 cites W2084462514 @default.
- W2017847493 cites W2088381734 @default.
- W2017847493 cites W2097998476 @default.
- W2017847493 cites W2105319189 @default.
- W2017847493 cites W2109147918 @default.
- W2017847493 cites W2111198076 @default.
- W2017847493 cites W2118015101 @default.
- W2017847493 cites W2124028893 @default.
- W2017847493 cites W2142637881 @default.
- W2017847493 cites W2145020331 @default.
- W2017847493 cites W2322411468 @default.
- W2017847493 cites W2500210460 @default.
- W2017847493 cites W2949648252 @default.
- W2017847493 cites W2950691457 @default.
- W2017847493 cites W4211210100 @default.
- W2017847493 doi "https://doi.org/10.1002/cjoc.201090012" @default.
- W2017847493 hasPublicationYear "2009" @default.
- W2017847493 type Work @default.
- W2017847493 sameAs 2017847493 @default.
- W2017847493 citedByCount "7" @default.
- W2017847493 countsByYear W20178474932012 @default.
- W2017847493 countsByYear W20178474932013 @default.
- W2017847493 countsByYear W20178474932014 @default.
- W2017847493 countsByYear W20178474932015 @default.
- W2017847493 crossrefType "journal-article" @default.
- W2017847493 hasAuthorship W2017847493A5025989570 @default.
- W2017847493 hasAuthorship W2017847493A5033848839 @default.
- W2017847493 hasAuthorship W2017847493A5038336511 @default.
- W2017847493 hasAuthorship W2017847493A5044933041 @default.
- W2017847493 hasAuthorship W2017847493A5073284317 @default.
- W2017847493 hasConcept C131779359 @default.
- W2017847493 hasConcept C155647269 @default.
- W2017847493 hasConcept C178790620 @default.
- W2017847493 hasConcept C185592680 @default.
- W2017847493 hasConcept C2776701986 @default.
- W2017847493 hasConcept C2776730309 @default.
- W2017847493 hasConcept C2779248272 @default.
- W2017847493 hasConcept C2780263894 @default.
- W2017847493 hasConcept C2780471494 @default.
- W2017847493 hasConcept C2781014771 @default.
- W2017847493 hasConcept C2781283055 @default.
- W2017847493 hasConcept C4937899 @default.
- W2017847493 hasConcept C544956773 @default.
- W2017847493 hasConcept C55493867 @default.
- W2017847493 hasConceptScore W2017847493C131779359 @default.
- W2017847493 hasConceptScore W2017847493C155647269 @default.
- W2017847493 hasConceptScore W2017847493C178790620 @default.
- W2017847493 hasConceptScore W2017847493C185592680 @default.
- W2017847493 hasConceptScore W2017847493C2776701986 @default.
- W2017847493 hasConceptScore W2017847493C2776730309 @default.
- W2017847493 hasConceptScore W2017847493C2779248272 @default.
- W2017847493 hasConceptScore W2017847493C2780263894 @default.
- W2017847493 hasConceptScore W2017847493C2780471494 @default.
- W2017847493 hasConceptScore W2017847493C2781014771 @default.
- W2017847493 hasConceptScore W2017847493C2781283055 @default.
- W2017847493 hasConceptScore W2017847493C4937899 @default.
- W2017847493 hasConceptScore W2017847493C544956773 @default.
- W2017847493 hasConceptScore W2017847493C55493867 @default.
- W2017847493 hasIssue "12" @default.
- W2017847493 hasLocation W20178474931 @default.
- W2017847493 hasOpenAccess W2017847493 @default.
- W2017847493 hasPrimaryLocation W20178474931 @default.
- W2017847493 hasRelatedWork W1542701265 @default.
- W2017847493 hasRelatedWork W1566639232 @default.
- W2017847493 hasRelatedWork W2019262624 @default.
- W2017847493 hasRelatedWork W2062651388 @default.
- W2017847493 hasRelatedWork W2092430625 @default.
- W2017847493 hasRelatedWork W2099995806 @default.
- W2017847493 hasRelatedWork W2580301023 @default.
- W2017847493 hasRelatedWork W2950850432 @default.
- W2017847493 hasRelatedWork W4243806292 @default.
- W2017847493 hasRelatedWork W8491676 @default.
- W2017847493 hasVolume "27" @default.
- W2017847493 isParatext "false" @default.
- W2017847493 isRetracted "false" @default.
- W2017847493 magId "2017847493" @default.
- W2017847493 workType "article" @default.