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- W2017932322 abstract "A route to fluvirucinins B2−5 (the common aglycon of fluvirucins B2−B5, Sch 38518, and Sch 39185) is reported for the first time. A ring-closing metathesis (RCM) generated the C6−C7 double bond, which by catalytic hydrogenation (in toluene) gave the desired epimer with a 9:1 diastereoselection. Azide 8a and carboxylic acid 5 came from ethyl-branched fragments C9−C13 (CHO at C9) and C1−C5 via an asymmetric allylation of the former and a cross metathesis (CM) followed by a ketone methylenation (with 20 mol % of DMF as a sacrificial additive) of the latter." @default.
- W2017932322 created "2016-06-24" @default.
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- W2017932322 creator A5051810560 @default.
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- W2017932322 date "2009-07-07" @default.
- W2017932322 modified "2023-10-18" @default.
- W2017932322 title "Efficient Approach to Fluvirucins B<sub>2</sub>−B<sub>5</sub>, Sch 38518, and Sch 39185. First Synthesis of their Aglycon, via CM and RCM Reactions" @default.
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- W2017932322 doi "https://doi.org/10.1021/ol901030f" @default.
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