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- W2017946539 abstract "A facile synthetic scheme for the preparation of methyl 4-deoxy-β-l-threo-hex-4-enopyranosiduronic acid utilizing the commercially available methyl α-d-galactopyranoside as starting material has been developed. The synthesis sequence comprises six high yielding reaction steps: TEMPO oxidation, acetylation, methanolysis of the lactone, acetylation, β-elimination, and final removal of the protecting groups. Only one column chromatographic purification is needed throughout the whole sequence. The overall yield is 60%. The final product has been characterized by NMR, Raman, UVRR, FTIR, and HRMS." @default.
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- W2017946539 date "2006-10-01" @default.
- W2017946539 modified "2023-10-09" @default.
- W2017946539 title "Synthesis and characterization of the hexenuronic acid model methyl 4-deoxy-β-l-threo-hex-4-enopyranosiduronic acid" @default.
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- W2017946539 doi "https://doi.org/10.1016/j.carres.2006.06.012" @default.
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