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• W2018123425 startingPage "221" @default.
• W2018123425 abstract "Thermal transformations of natural calcium oxalate dihydrate known in mineralogy as weddellite have been undertaken using a combination of Raman microscopy and infrared emission spectroscopy. The vibrational spectroscopic data was complimented with high resolution thermogravimetric analysis combined with evolved gas mass spectrometry. TG–MS identified three mass loss steps at 114, 422 and 592 °C. In the first mass loss step water is evolved only, in the second and third steps carbon dioxide is evolved. The combination of Raman microscopy and a thermal stage clearly identifies the changes in the molecular structure with thermal treatment. Weddellite is the phase in the temperature range up to the pre-dehydration temperature of 97 °C. At this temperature, the phase formed is whewellite (calcium oxalate monohydrate) and above 114 °C the phase is the anhydrous calcium oxalate. Above 422 °C, calcium carbonate is formed. Infrared emission spectroscopy shows that this mineral decomposes at around 650 °C. Changes in the position and intensity of the CO and CC stretching vibrations in the Raman spectra indicate the temperature range at which these phase changes occur." @default.
• W2018123425 created "2016-06-24" @default.
• W2018123425 creator A5006496281 @default.
• W2018123425 creator A5051349883 @default.
• W2018123425 date "2003-11-01" @default.
• W2018123425 modified "2023-09-30" @default.
• W2018123425 title "Thermal treatment of weddellite—a Raman and infrared emission spectroscopic study" @default.
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• W2018123425 doi "https://doi.org/10.1016/s0040-6031(03)00259-4" @default.
• W2018123425 hasPublicationYear "2003" @default.
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