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- W2018163978 abstract "TiO 2 nanoparticles were synthesized by self-hydrolysis of TiOCl 2 using conventional and microwave heating methods. By XRD analysis, rutile and anatase phases were detected at the early stage of reaction. In conventional heating method, the XRD peaks of rutile became stronger with time and the roundish agglomerates surrounded by acicular particles were observed by SEM. The initial product was confirmed by TEM to consist of small acicular particles assigned to rutile and fine nanoparticles assigned to hydrous TiO 2 sol having anatase-like structure. As the reaction time was longer, the amount of acicular particles increased. These results suggest that TiO 2 sol formed at the early stage by hydrolysis of TiOCl 2 and the crystal growth of rutile progressed by dissolution-reprecipitation of TiO 2 sol. In order to synthesize TiO 2 nanoparticles, microwave was applied to this system. The microwave irradiation shortened the period of the precipitation because microwave can quickly heat up the aqueous solution, but retarded the crystal growth of rutile, leading to size reduction of TiO 2 particles identified a hydrous TiO 2 phase." @default.
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- W2018163978 date "2006-01-01" @default.
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- W2018163978 title "Microwave Effect for Synthesis of TiO2 Particles by Self-Hydrolysis of TiOCl2" @default.
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- W2018163978 doi "https://doi.org/10.2109/jcersj.114.814" @default.
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