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- W2018213613 abstract "Crystal structure of the low temperature form of LiMn2O4 has been successfully determined by using single-crystal X-ray diffraction data at 130 K. It belongs to the orthorhombic system, space group Fddd with a=24.750(3) Å, b=24.801(2) Å, c=8.1903(9) Å, and V=5027.4(9) Å3. The structure, including anisotropic displacement parameters for each atom, was refined to the conventional values R1=5.58%, wR2=7.16%, and S=1.180 for 8082 independent reflections. The oxygen sublattice deformation toward the [1 1 0] direction in the low temperature form is clearly observed at 130 K. The structural phase transition around 280 and 320 K was precisely examined by differential scanning calorimetry (DSC) and single-crystal X-ray diffraction measurements using the single-crystal samples." @default.
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- W2018213613 date "2004-08-01" @default.
- W2018213613 modified "2023-10-17" @default.
- W2018213613 title "Single-crystal X-ray structure analysis of the low temperature form of LiMn2O4" @default.
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- W2018213613 doi "https://doi.org/10.1016/j.ssi.2004.01.051" @default.
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