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- W2018255035 abstract "A heterometallic hexameric germanotungstate containing iron–lanthanide cluster fragments (enH2)13HK9[Fe6Sm6(H2O)12(α-GeW10O38)6]·42H2O (1) and a hexairon substituted double sandwich-type germanotungstate (enH2)6K[HFe6(B-α-GeW9O34)2(α-GeW6O26)(H2O)2]·11H2O (2) (en = 1,2-ethylenediamine) have been hydrothermally synthesized and structurally characterized using elemental analyses, inductively coupled plasma atomic emission spectrometry, IR spectra, powder X-ray diffraction (PXRD), thermogravimetric (TG) analyses and single-crystal X-ray diffraction. The common features of 1 and 2 are that both are based on lacunary Keggin-type germanotungstate fragments. 1 is the first heterometallic hexameric germanotungstate consisting of six {Fe–(μ3-O)3–Sm} bridges, while two double sandwich-type fragments in 2 are connected together through two potassium cations forming hexameric germanotungstate units. The magnetic susceptibility measurements demonstrate the presence of antiferromagnetic interactions in both compounds." @default.
- W2018255035 created "2016-06-24" @default.
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- W2018255035 date "2014-01-01" @default.
- W2018255035 modified "2023-09-29" @default.
- W2018255035 title "Syntheses, structures and properties of two multi-iron–samarium/multi-iron substituted germanotungstates" @default.
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- W2018255035 doi "https://doi.org/10.1039/c3ce42023j" @default.
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