Matches in SemOpenAlex for { <https://semopenalex.org/work/W2018268462> ?p ?o ?g. }
Showing items 1 to 80 of
80
with 100 items per page.
- W2018268462 endingPage "1324" @default.
- W2018268462 startingPage "1318" @default.
- W2018268462 abstract "Incubation of fumonisin B(1) and D-glucose in aqueous solutions resulted in the formation of N-(1-deoxy-D-fructos-1-yl) fumonisin B(1) in addition to the previously reported N-(carboxymethyl) fumonisin B(1). N-(1-Deoxy-D-fructos-1-yl) fumonisin B(1) is the first stable product formed after the Amadori rearrangement of the Schiff base formed by the reaction of the primary amine of fumonisin B(1) and the aldehyde group of D-glucose. N-(1-Deoxy-D-fructos-1-yl) fumonisin B(1) was synthesized by reacting fumonisin B(1) with an excess of D-glucose in methanol and heating for 6 h at 64 degrees C. It was purified using C(18) and strong cation exchange solid-phase extraction cartridges and characterized by nuclear magnetic resonance and liquid chromatography-mass spectrometry. Subsequently, N,N-dimethylformamide was found to be a better reaction solvent, requiring reaction for only 2-3 h at 64 degrees C and eliminating the formation of methyl esters. Alkaline hydrolysis of N-(1-deoxy-D-fructos-1-yl) fumonisin B(1) gave a mixture of hydrolyzed fumonisin B(1) and hydrolyzed N-(carboxymethyl) fumonisin B(1)." @default.
- W2018268462 created "2016-06-24" @default.
- W2018268462 creator A5007568131 @default.
- W2018268462 creator A5016438683 @default.
- W2018268462 creator A5078814471 @default.
- W2018268462 date "2002-01-25" @default.
- W2018268462 modified "2023-10-03" @default.
- W2018268462 title "<i>N</i>-(1-Deoxy-<scp>d</scp>-fructos-1-yl) Fumonisin B<sub>1</sub>, the Initial Reaction Product of Fumonisin B<sub>1</sub> and <scp>d</scp>-Glucose" @default.
- W2018268462 cites W139903017 @default.
- W2018268462 cites W1577347418 @default.
- W2018268462 cites W1971291583 @default.
- W2018268462 cites W1971442391 @default.
- W2018268462 cites W1974660033 @default.
- W2018268462 cites W1998243002 @default.
- W2018268462 cites W2006954456 @default.
- W2018268462 cites W2007506045 @default.
- W2018268462 cites W2072607078 @default.
- W2018268462 cites W2116103262 @default.
- W2018268462 cites W2167212778 @default.
- W2018268462 cites W2177161308 @default.
- W2018268462 cites W2322220130 @default.
- W2018268462 cites W2486435436 @default.
- W2018268462 cites W2527629139 @default.
- W2018268462 cites W642247737 @default.
- W2018268462 doi "https://doi.org/10.1021/jf010955g" @default.
- W2018268462 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/11853524" @default.
- W2018268462 hasPublicationYear "2002" @default.
- W2018268462 type Work @default.
- W2018268462 sameAs 2018268462 @default.
- W2018268462 citedByCount "52" @default.
- W2018268462 countsByYear W20182684622012 @default.
- W2018268462 countsByYear W20182684622014 @default.
- W2018268462 countsByYear W20182684622015 @default.
- W2018268462 countsByYear W20182684622017 @default.
- W2018268462 countsByYear W20182684622018 @default.
- W2018268462 countsByYear W20182684622019 @default.
- W2018268462 countsByYear W20182684622020 @default.
- W2018268462 countsByYear W20182684622021 @default.
- W2018268462 countsByYear W20182684622022 @default.
- W2018268462 countsByYear W20182684622023 @default.
- W2018268462 crossrefType "journal-article" @default.
- W2018268462 hasAuthorship W2018268462A5007568131 @default.
- W2018268462 hasAuthorship W2018268462A5016438683 @default.
- W2018268462 hasAuthorship W2018268462A5078814471 @default.
- W2018268462 hasConcept C178790620 @default.
- W2018268462 hasConcept C185592680 @default.
- W2018268462 hasConcept C2778431908 @default.
- W2018268462 hasConcept C2781429003 @default.
- W2018268462 hasConcept C31903555 @default.
- W2018268462 hasConcept C84699730 @default.
- W2018268462 hasConcept C94412978 @default.
- W2018268462 hasConceptScore W2018268462C178790620 @default.
- W2018268462 hasConceptScore W2018268462C185592680 @default.
- W2018268462 hasConceptScore W2018268462C2778431908 @default.
- W2018268462 hasConceptScore W2018268462C2781429003 @default.
- W2018268462 hasConceptScore W2018268462C31903555 @default.
- W2018268462 hasConceptScore W2018268462C84699730 @default.
- W2018268462 hasConceptScore W2018268462C94412978 @default.
- W2018268462 hasIssue "5" @default.
- W2018268462 hasLocation W20182684621 @default.
- W2018268462 hasLocation W20182684622 @default.
- W2018268462 hasOpenAccess W2018268462 @default.
- W2018268462 hasPrimaryLocation W20182684621 @default.
- W2018268462 hasRelatedWork W1970144168 @default.
- W2018268462 hasRelatedWork W1988672645 @default.
- W2018268462 hasRelatedWork W2081391750 @default.
- W2018268462 hasRelatedWork W2095581038 @default.
- W2018268462 hasRelatedWork W2316939667 @default.
- W2018268462 hasRelatedWork W2326430580 @default.
- W2018268462 hasRelatedWork W2403182174 @default.
- W2018268462 hasRelatedWork W2467741287 @default.
- W2018268462 hasRelatedWork W2472796425 @default.
- W2018268462 hasRelatedWork W2558998514 @default.
- W2018268462 hasVolume "50" @default.
- W2018268462 isParatext "false" @default.
- W2018268462 isRetracted "false" @default.
- W2018268462 magId "2018268462" @default.
- W2018268462 workType "article" @default.