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• W2018325868 abstract "The new oligophosphines [H2P(CH2)2]2PH, [H2P(CH2)2P(H)CH2]2, and{[(H2P(CH2)2]2PCH2}2 have been made by hydrophosphination of diethyl vinylphosphonate (2) with H2P(CH2)2PH2 (1), using different ratios of 2/1, followed by LiAlH4 reduction of the phosphonate intermediates; the three phosphonate precursors were obtained as oils of varying purity (approximately 90-95%) in low (approximately 20%) to almost quantitative yield. The tri-, tetra-, and hexaphosphines were then treated with formaldehyde in the presence of hydrochloric acid to generate the corresponding water-soluble (hydroxymethyl)phosphonium chlorides {(HOCH2)3P[(CH2)2P(CH2OH)2]n(CH2)2P(CH2OH)3}Cl m (n = 1, m = 3; n = 2, m = 4) and {[(HOCH2)3P(CH2)2]2P(CH2OH)CH2}2Cl6 that were characterized by NMR spectroscopy and elemental analysis. The known (hydroxymethyl)bisphosphonium chloride [(HOCH2)3P(CH2)2]2Cl2 was similarly prepared from H2P(CH2)2PH2, and the determined crystal structure revealed strong hydrogen bonding between the chloride anions and the hydrogen atoms of the hydroxymethyl groups." @default.
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• W2018325868 date "2006-02-28" @default.
• W2018325868 modified "2023-10-06" @default.
• W2018325868 title "New Oligophosphines and (Hydroxymethyl)phosphonium Chlorides" @default.
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• W2018325868 doi "https://doi.org/10.1021/ic0518935" @default.
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