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• W2018351106 abstract "The new ionic plastic crystals N,N-dimethylpyrrolidinium fluorohydrogenate [DMPyr(FH)2F] and N-ethyl-N-methylpyrrolidinium fluorohydrogenate [EMPyr(FH)2F] were prepared, and their physicochemical, structural, and electrochemical properties were investigated. The DMPyr(FH)2F and EMPyr(FH)2F salts exhibited small entropy changes of melting, 4.1 and 2.0 J K–1 mol–1, respectively, and had ionic plastic crystal phases in the temperature ranges of 258–325 and 236–303 K, respectively. These phases had NaCl-type structures; the lattice constants were 9.90 Å for DMPyr(FH)2F and 10.18 Å for EMPyr(FH)2F. The ionic conductivities of the ionic plastic crystal phases ranged from 100 to 101 mS cm–1 [e.g., 10.3 mS cm–1 at 298 K for DMPyr(FH)2F and 14.4 mS cm–1 at 288 K for EMPyr(FH)2F]. Pulsed-field gradient spin–echo NMR spectroscopy revealed that only the anion could move in the ionic plastic crystal phase as a charge carrier with a diffusion coefficient of ∼10–7 cm2 s–1. The self-diffusion coefficient of the cation in the ionic plastic crystal phase of DMPyr(FH)2F was too small to measure, although the cation in EMPyr(FH)2F had a slight mobility below 303 K." @default.
• W2018351106 created "2016-06-24" @default.
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• W2018351106 date "2013-01-10" @default.
• W2018351106 modified "2023-09-25" @default.
• W2018351106 title "Highly Conductive Plastic Crystals Based on Fluorohydrogenate Anions" @default.
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• W2018351106 doi "https://doi.org/10.1021/jp311558h" @default.
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