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- W2018352302 abstract "The feasibility of using reversed-phase liquid chromatography/mass spectrometry (LC/MS) with an electrospray (ES) interface for measuring traces of N-methylcarbamate insecticides in 10 different types of fruits and vegetables was evaluated. Twelve carbamates added to vegetable materials were extracted with methanol by the aid of a homogenizer. After filtration, an aliquot of the homogenizate equivalent to 5 g of the vegetable material was suitably diluted with water and passed through a 1-g Carbograph 1 extraction cartridge. Carbamates were eluted by passing through the cartridge 6 mL of a CH2Cl2/CH3OH (80:20 v/v) mixture. After eluate concentration down to 100 μL, 5 μL of the final extact was injected into the LC column. Recovery of the analytes was better than 80%, irrespective of the type of vegetable matrix to which the analytes were added. Replacement of CH3OH with CH3CN as organic modifier resulted in a significant decrease of the ion signal for carbamates. The same occurred by adding moderate amoun..." @default.
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- W2018352302 title "Evaluation of a Method Based on Liquid Chromatography/Electrospray/Mass Spectrometry for Analyzing Carbamate Insecticides in Fruits and Vegetables" @default.
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- W2018352302 doi "https://doi.org/10.1021/jf950779+" @default.
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