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- W2018382603 abstract "MoTe4Br is obtained from Te2Br and MoTe2in a sealed evacuated silica ampoule at 440°C in the form of platelike crystals with a silver luster. It crystallizes in the triclinic space groupP1 witha= 682.1(3) pm,b= 783.6(3) pm,c= 793.1(3) pm, α = 113.25(2)°, β = 102.97(1)°, γ = 101.37(2)°. The structure is built of infinite one-dimensional Mo(Te2)2chains with intercalated bromide ions and Mo2pair formation along the chain. MoTe6Br3is formed from MoBr3, Te2Br, and Te in 1:2:2 molar ratio in a sealed evacuated glass ampoule at 300°C. The silvery crystals belong to the triclinic crystal system, space groupP1,a= 837.2(1) pm,b= 1141.4(2) pm,c= 1442.0(2) pm, α = 81.70(1)°, β = 83.07(1)°, γ = 74.34(1)°. The structure consists of dimeric cationic complexes [Mo2(Te2)2(Te4)2]6+which are connected by bromide ions to layers. In the complexes Mo2pairs are bridged by two Te2−2groups and are additionally bound in a η4–π fashion to two almost planar Te4rings that can be considered to be Te2+4polycations. The complexes in the structure of MoTe6Br3can formally be derived as fragments from the chains of MoTe4Br." @default.
- W2018382603 created "2016-06-24" @default.
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- W2018382603 date "1996-09-01" @default.
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- W2018382603 title "Mo2Dimers in [Mo(Te2)2] Chains in MoTe4Br and in their Cationic Fragments [Mo2(Te2)2(Te4)2]6+in MoTe6Br3: Two Molybdenum Telluride Bromides with a Close Structural Relationship" @default.
- W2018382603 doi "https://doi.org/10.1006/jssc.1996.0280" @default.
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