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- W2018384013 abstract "A New Synthetic Way to the Tetracyclic Skeleton of Cyclohepta ( def )fluorene The synthesis of 2‐Methyl‐4, 5, 6, 8, 9, 10‐hexahydrocyclohepta ( def )fluorene 2 is described starting with the reduction of the ketone 3 by a (1:1)‐mixture of LiAlH 4 /AlCl 3 to the hydrocarbon 4 . After metallation with butyllithium 4 was allowed to react with bromoacetic acid to yield 5 . The cyclization of this compound was performed with p ‐toluenesulfonic acid to give the tetracyclic ketone 6 which was converted to the tetracyclic hydrocarbon 2 by reduction with LiAlH 4 /AlCl 3 ." @default.
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- W2018384013 date "1981-04-29" @default.
- W2018384013 modified "2023-09-30" @default.
- W2018384013 title "Ein neuer Zugang zum tetracyclischen Grundgerüst des Cyclohepta (<i>def</i>)fluorens" @default.
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- W2018384013 doi "https://doi.org/10.1002/hlca.19810640329" @default.
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