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- W2018411931 abstract "The synthesis of 15-N-acetylglucosaminides of 15α-hydroxyestrone, 15α-hydroxyestradiol, and 15α-hydroxyestriol (estetrol) is described. The latter two were prepared by condensation of 2-acetamido-1α-chloro1,2-dideoxy-3,4,6-trio-O-acetyl-d-glucopyranose with appropriately protected 15α-hydroxyestrogens by the Koenigs-Knorr reaction employing cadmium carbonate as a catalyst. Subsequent removal of protecting groups with methanolic potassium hydroxide provided the desired conjugates. 15α-Hydroxyestrone 15-N-acetylglucosaminide was synthesized from the corresponding 15α-hydroxyestradiol derivative by Jones oxidation followed by brief alkaline hydrolysis. These conjugates underwent enzymatic hydrolysis with β-N-acetylgucosaminidase from Jack beans to produce 15α-hydroxyestrogens." @default.
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- W2018411931 date "1995-03-01" @default.
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- W2018411931 title "Synthesis of 15α-hydroxyestrogen 15-N-acetylglucosaminides" @default.
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- W2018411931 doi "https://doi.org/10.1016/0039-128x(94)00054-g" @default.
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