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• W2018432800 abstract "Pure lead titanate (PbTiO3) crystals (5 x 5 x 5 mm3) were grown from high-temperature solutions by a slow cooling technique using PbO as a self-flux. The optimum growth conditions were determined to be: (1) (1-x) TiO2 + x PbO with x (in moi%) varying from 0.78 to 0.82 for the starting compositions, (2) 930-1050°C as the growth temperature range and (3) 0.4-1.5°C/h as the cooling rates. Evaporation of PbO was significantly reduced by use of a double-crucible technique. The grown crystals were characterized by X-ray diffraction, chemical analysis and optical microscopy. The transformation temperatures (onset) of 492.5°C (on heating) and 491.3°C (on cooling) were determined by differential scanning calorimetry. The transformation process had a thermal hysteresis of 1.2°C from onset data." @default.
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• W2018432800 date "1993-03-01" @default.
• W2018432800 modified "2023-09-27" @default.
• W2018432800 title "Growth of large PbTiO3 crystals by a self-flux technique" @default.
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• W2018432800 doi "https://doi.org/10.1016/s0022-0248(07)80060-1" @default.
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