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• W2018498105 abstract "Solid state 11B, 27Al and 31P nuclear magnetic resonance spectroscopy has been used to study the microstructure of 16 Al2O3B2O3P2O5 glasses whose constituents may all act as glass formers. To obtain the fundamental parameters for the quadrupolar 27Al nuclei satellite transition spectroscopy has been applied. As a result, boron occurs always four-coordinated, while aluminium atoms are distinguished by three well defined environments assigned to four-, five- and six-coordination; the proportion of four-coordinated Al species decreases with increasing P2O5 content, that of five- and six-coordinated species increases. Phosphorus is tetrahedrally coordinated, its chemical shift varies systematically as a function of the bonding behavior in the second coordination sphere. The experimental findings can be described by a random network model for the whole glass-forming region, which includes a continuous transition from a silica-like structure of AlPO4 and BPO4 for [P2O5]/([B2O3] + [Al2O3(4)]) ratios of about 1, to a more loosened structure containing AlO4, AlO5 as well as Al(PO3)3 elements, if there is excess oxygen and this ratio becomes larger." @default.
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• W2018498105 date "1996-12-01" @default.
• W2018498105 modified "2023-10-17" @default.
• W2018498105 title "Multinuclear MAS-NMR studies of Al2O3B2O3P2O5 glasses" @default.
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• W2018498105 doi "https://doi.org/10.1016/s0022-3093(96)00522-4" @default.
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