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- W2018510299 abstract "Using tris(2-ethylamino)amine (tren) as a template, three new fluorides are obtained by solvothermal synthesis: [(C2H4NH3)3NH]·[Zr3F16(H2O)] (I), [(C2H4NH3)3N]2·[ZrF6]·[Zr2F12] (II) and [(C2H4NH3)3N]·[TaF7]·F (III). The structure determinations are performed by single crystal technique. The structure of I consists of infinite spiral-like [Zr3F16(H2O)]4− chains connected by tetraprotonated [trenH4]4+ cations which possess a plane configuration. In II, isolated [ZrF6] octahedra or [Zr2F12] dimers are linked to organic cations by a tridimensional hydrogen bond network. In III, [TaF7]2− monocapped trigonal prisms and “isolated” fluoride ions are connected by hydrogen bonds to template moieties. In II and III, every organic moiety is triprotonated [trenH3]3+ with a “spider” configuration. In the tantalum phase, the hydrogen bond network leads to the formation of a layered structure." @default.
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- W2018510299 date "2004-11-01" @default.
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- W2018510299 title "Tris(2-ethylamino)amine (tren) as template for the elaboration of fluorides: synthesis and crystal structures of [(C2H4NH3)3NH]·[Zr3F16(H2O)], [(C2H4NH3)3N]2·[ZrF6]·[Zr2F12] and [(C2H4NH3)3N]·[TaF7]·F" @default.
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- W2018510299 doi "https://doi.org/10.1016/j.jssc.2004.07.051" @default.
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