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- W2018532818 abstract "The deuteron quadrupole coupling constants and asymmetry factors in single crystals of DCOOH and HCOOD are found to be 161± 2 kHz, η=0.040± 0.025 and 165.1± 2.7 kHz, η=0.125± 0.030, respectively. These are compared with free molecule and single crystal results of others on the formate group. In addition, attention is called to influence of the X-fragment electronegativity upon the deuteron coupling constant in C–DX compounds with sp2 hybridization. The temperature independent CD3COOH results, 58± 2 kHz, η ≤ 0.1, indicate rapid hindered rotation of the CD3 group, with correlation time τ ≲ 2(10−8) sec, above 63°K. This result is shown to be in good agreement with the only other single crystal result available for sp3 hybridized deuterocarbon compounds, i.e., malonic acid." @default.
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- W2018532818 date "1972-02-01" @default.
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- W2018532818 title "Deuteron NMR in Formic and Acetic Acid Single Crystals" @default.
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- W2018532818 doi "https://doi.org/10.1063/1.1677349" @default.
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