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- W2018576043 abstract "Transmission electron microscopy (TEM), electron diffraction (ED), and electron density maps (EDM) experiments were carried out on a poly[N-[3,4,5-tris(n-dodecan-1-yloxy)benzoyl]ethyleneimine] [poly[(3,4,5)12G1-Oxz]] with a degree of polymerization (DP) of 20. All experiments confirmed the thermotropic body-centered cubic (BCC) Im3m lattice suggested previously by X-ray diffraction (XRD) experiments. The unit cell parameter determined by ED at 23 degrees C is a = 42.4 A, in good agreement with XRD results which show a = 42.6 A after quenching from 70 degrees C. EDM of the XRD results confirm that the supramolecular minidendrimer obtained from poly[(3,4,5)12G1-Oxz] adopts a spherical inverse micellar-like structure, with the polyethyleneimine backbone and the aromatic groups microsegregated and concentrated in the corners and in the center of the cubic unit cell. A space-filling continuum is realized by the n-alkyl groups that radiate out of the aromatic core of the spherical dendrimer. This manuscript is only the second example of complete structural analysis of a lattice generated from supramolecular objects and complements the previous example reported from our laboratory on the Pm3n lattice." @default.
- W2018576043 created "2016-06-24" @default.
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- W2018576043 date "2001-10-01" @default.
- W2018576043 modified "2023-10-15" @default.
- W2018576043 title "Definitive Support by Transmission Electron Microscopy, Electron Diffraction, and Electron Density Maps for the Formation of a BCC Lattice from Poly{N-[3,4,5-tris(n-dodecan-l-yloxy)benzoyl]ethyleneimine}" @default.
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- W2018576043 doi "https://doi.org/10.1002/1521-3765(20011001)7:19<4134::aid-chem4134>3.0.co;2-w" @default.
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