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- W2018678591 abstract "Abstract A mixture of products from the oxidative dehydrogenation of isobutene to methacrolein has been separated into two parts. The first, the absorbate, consists mainly of aldehydes, and the second, the condensate, consists mainly of acids. The main purpose of the present work was the application of gas—liquid chromatography (GLC) or its combination with mass spectrometry (MS) to the identification of the reaction products. Using PEG 400 plus PEG 3000 as a stationary phase, twelve components were identified in the absorbate by means of GLC-MS. Quantitative determination using the method of internal standards showed that the absorbate consists mainly of acetaldehyde, acetone and methacrolein in addition to an excess of water. In the condensate, using Reoplex 400 plus orthophosphoric acid on Chromosorb W, twenty-four compounds were identified. The main part of the condensate is water, and of the other compounds the main ones are acetic acid, methacrylic acid and methacrolein." @default.
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- W2018678591 date "1972-02-01" @default.
- W2018678591 modified "2023-09-23" @default.
- W2018678591 title "Determination of products from the oxidative dehydration of isobutene by gas—liquid chromatography—mass spectrometry" @default.
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- W2018678591 doi "https://doi.org/10.1016/s0021-9673(00)86945-9" @default.
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