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- W2018694003 abstract "Abstract The complexes trans -[Ru(dppm) 2 (CCPh 2 ] and trans -[Ru(LL) 2 CCRCC] n − [LL = bis-diphenylphosphino)methane (dppm) or bis-(diphenylphosphino)ethane (dppe), R = p -C 6 H 4 or p -C 6 H 2 (CH 3 ) 2 ] have geen prepared by the reaction of the corresponding trans -[Ru(LL) 2 Cl 2 ] compound with Me 3 SnCCPh or Me 3 SnCCRCCSnMe 3 . Reactions between cis -[Ru(LL) 2 Cl 2 ], acetylenes and the salt NaPF 6 have yielded complexes of the type [CI(LL) 2 RuCCPhH] + PF 6 − . These were converted into the corresponding mono-acetylides, [Ru(LL) 2 Cl(CCPh)] by treatment with 1,8-diazabicyclo[5.4. Ojundec-7-ene(DBU) or alumina. Ale single crystal X-ray structure of [Ru(dppe) 2 Cl(CCPh)] confirms that during the reaction of the cis -dihalide species rearrangement takes place to give trans products." @default.
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- W2018694003 date "1994-11-01" @default.
- W2018694003 modified "2023-10-17" @default.
- W2018694003 title "Ruthenium(II) σ-acetylide complexes; monomers, dimers and polymers" @default.
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- W2018694003 doi "https://doi.org/10.1016/0022-328x(94)88195-2" @default.
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