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• W2018797142 endingPage "1463" @default.
• W2018797142 startingPage "1453" @default.
• W2018797142 abstract "The solution structure of the DNA decamer (CATGGCCATG)2 has been determined by NMR spectroscopy and restrained molecular dynamic and distance geometry calculations. The restrainted data set includes interproton distances and torsion angles for the deoxyribose sugar ring which were obtained by nuclear Overhauser enhancement intensities and quantitative simulation of cross-peaks from double quantum filtered correlation spectroscopy. The backbone torsion angles were constrained using experimental data from NOE cross-peaks, 1H-1H and 1H-31P-coupling constants. The NMR structure and the crystal structure of the DNA decamer deviates from the structure of the canonical form of B-DNA in a number of observable characteristics. Particularly, both structures display a specific pattern of stacking interaction in the central GGC base triplet. Furthermore, a specific local conformation of the TG/CA base-pair step is present in NMR and crystal structure, highlighting the unusually high flexibility of this DNA duplex part. The solution structure of the TG/CA base-pair step obtained by our high resolution NMR study is characterized by a positive roll angle, whereas in crystal this base-pair step tends to adopt remarkably high twist angles." @default.
• W2018797142 created "2016-06-24" @default.
• W2018797142 creator A5007623203 @default.
• W2018797142 creator A5039301125 @default.
• W2018797142 creator A5063756937 @default.
• W2018797142 date "1998-12-01" @default.
• W2018797142 modified "2023-09-23" @default.
• W2018797142 title "Structure determination and analysis of helix parameters in the DNA decamer d(CATGGCCATG) 2 comparison of results from NMR and crystallography 1 1Edited by I. Tinoco" @default.
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• W2018797142 doi "https://doi.org/10.1006/jmbi.1998.2261" @default.
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