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• W2018869968 abstract "Direct analysis in real time (DART) ionisation coupled to mass spectrometry (MS) was used for the rapid quantitative analysis of T-2 toxin (T-2) and the related HT-2 toxin (HT-2), extracted from maize. Sample preparation procedures and instrument parameters were optimised to obtain sensitive and accurate determination of the toxins. The lowest calibration levels were 50 μg/kg for T-2 and 300 μg/kg for HT-2. Quantitative analysis was performed with the use of matrix-matched standards employing the 13 C-labelled internal standard for T-2. DART-MS of maize extracts spiked with T-2 gave a linear response over the range of 50-1000 μg/kg. With the isotope dilution technique, good recoveries (99-110%) and repeatabilities (relative standard deviaiton 7.4-11.6%) were obtained at T-2 spiking levels of 100 and 1000 μg/kg. Adaptability of the developed method was demonstrated by analysis of T-2 and HT-2 from an oat flour quality control material. The results here further indicate the potential for application of ambient ionisation mass spectrometry to provide accurate, convenient quantitation of mycotoxins from grains." @default.
• W2018869968 created "2016-06-24" @default.
• W2018869968 creator A5033030062 @default.
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• W2018869968 date "2015-08-17" @default.
• W2018869968 modified "2023-10-16" @default.
• W2018869968 title "Determination of T-2 and HT-2 toxins from maize by direct analysis in real time mass spectrometry" @default.
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• W2018869968 doi "https://doi.org/10.3920/wmj2014.1854" @default.
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