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- W2018908797 abstract "Abstract The interaction of the potentially pentadentate compartmental Schiff base, (H3L), derived by condensation of 2,6-diformyl-4-chlorophenol and o- aminophenol with thorium(IV) salts has been studied and the crystal structure of the ionic complex [Mg[Th2L3]2·6H2O determined by X-ray crystallography. The compound is monoclinic, space group P21/c, with a=12.488(6), b=22.044(5), c=24.316(5) A, and β=104.82(3)°; Dc=1.66 g cmt-3 for Z= 2. The structure was refined to the final conventional R of 0.067 based on 5455 observed reflexions. The two independent Th atoms of the monoanionic [Th2L3]− complex are nona-coordinate and bridged by three oxygen atoms. The Mg2+ cations, which are on crystallographic centres of symmetry, are octahedrally surrounded by H2O molecules. Selected bond distances are: ThO (bridging) 2.47 A (mean value), ThO 2.31 A (mean value), ThN 2.74 ) A (mean value), MgṫO 2.09 A (mean value)." @default.
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- W2018908797 date "1987-11-01" @default.
- W2018908797 modified "2023-10-18" @default.
- W2018908797 title "Preparation, characterization and crystal structure of a binuclear thorium(IV) complex with a pentadentate compartmental Schiff Base" @default.
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- W2018908797 doi "https://doi.org/10.1016/s0020-1693(00)84473-4" @default.
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