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- W2018946560 abstract "The retention of organic acids, amines, aminophenols, and amides was directly proportional to the surface area of Diol coated silica particles. Surface area was measured in situ using the method of Hong and Parcher [Anal. Chem., 62 (1990) 2313–2317]. Linear regression analysis was performed on the results from four pore diameters (100, 300, 500 and 4000), plus the origin. Correlation coefficients between retention and surface area were as high as 0.9991. Both the surface area of the chromatographic support and solute retention changed by more than 14 times. All the solutes tested behaved similarly, indicating that changing the surface area is a viable means of retention control. The smallest pore diameter tested (100 Å) produced the same efficiency as some of the larger pore sizes (i.e., 300 and 500 Å) suggesting that still smaller sizes, like 60 Å, might be useful for supercritical fluid chromatography. Particles with 4000 Å pores produced poor efficiency, due to peak tailing, which suggests that deactivation was inadequate." @default.
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- W2018946560 date "1992-03-01" @default.
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- W2018946560 title "Correlation between column surface area and retention of polar solutes in packed-column supercritical fluid chromatography" @default.
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- W2018946560 doi "https://doi.org/10.1016/0021-9673(92)80342-r" @default.
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