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- W2019005510 abstract "Dinuclear metal(II) complexes of 2,6-bis{N-[(2-dimethylamino)ethyl]iminomethyl}-4-methylphenol (HL), [Mn2(L)(AcO)2(NCS)] (1), [Co2(L)(AcO)2]BPh4 (2), [Ni2(L)(AcO)2(MeOH)]BPh4 (3), and [Zn2(L)(AcO)2]BPh4 (4), have been examined as regards their hydrolytic activity toward tris(p-nitrophenyl) phosphate (TNP) and hydrogen bis(p-nitrophenyl) phosphate (HBNP) by means of mass spectrometric methods as well as UV–visible spectroscopic methods. All the complexes hydrolyze TNP to BNP− in the relative activity of 4 > 2 > 1 >> 3. It is found that one AcO− group of [M2(L)(AcO)2]+ is replaced with BNP−, arising from the hydrolysis of TNP, affording [M2(L)(AcO)(bnp)]+ in an equilibrium with [M2(L)(AcO)2]+: [M2(L)(AcO)2]+ + BNP− [M2(L)(AcO)(bnp)]+ + AcO−. In the reaction of HBNP with 1–4, [M2(L)(AcO)(bnp)]+ is produced in the equilibrium with [M2(L)(AcO)2]+, and the bound BNP− is slowly hydrolyzed in the case of M = Mn and Co. The bound BNP− of [Ni2(L)(AcO)(bnp)]+ is barely hydrolyzed and the bound BNP− of [Zn2(L)(AcO)(bnp)]+ is practically not hydrolyzed. The relevance of the complexes to phosphotriesterase and phosphodiesterase is discussed." @default.
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- W2019005510 date "2005-10-01" @default.
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- W2019005510 title "Mass Spectrometric and Spectroscopic Studies on Hydrolysis of Phosphoesters by Bis(μ-acetato)-μ-phenolato Dinuclear Metal(II) Complexes (Metal = Mn, Co, Ni, and Zn)" @default.
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