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• W2019092712 abstract "A combinative method with three steps was developed to fabricate HNIW (2,4,6,8,10,12-hexanitro-2,4,6,8,10,12-hexaazaisowurtziane) nanoexplosives with the gas anti-solvent (GAS) method improved by introducing a gel frame to limit the overgrowth of recrystallized particles and an acid-assistant to remove the used frame. Forming the mixed gel, by locking the explosive solution into a wet gel whose volume was divided by the networks, was the key for the fabrication. As demonstrated by scanning electron microscopy (SEM) analysis, a log-normal size distribution of nano-HNIW indicated that about 74.4% of the particles had sizes <120 nm and maximum particle size was ∼300 nm. Energy-dispersive X-ray spectroscopy (EDS) and infrared (IR) characterizations showed that the aerogel embedded with nanoexplosive particles was dissolved in hydrochloric acid solution, and the raw ϵ-HNIW was mostly transformed into the α phase (nano-HNIW) during recrystallization. Nano-HNIW exhibited impact and friction sensitivity almost equal to those of raw HNIW, within experimental error. Thermal analysis showed that the decomposition peak temperature decreased by more than 10°C and that the heat release increased by 42.5% when the particle size of HNIW was at the nanometer scale." @default.
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• W2019092712 date "2013-01-01" @default.
• W2019092712 modified "2023-10-16" @default.
• W2019092712 title "A Versatile Methodology Using Sol-Gel, Supercritical Extraction, and Etching to Fabricate a Nitramine Explosive: Nanometer HNIW" @default.
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• W2019092712 doi "https://doi.org/10.1080/07370652.2011.633963" @default.
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