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• W2019166918 abstract "Conventional methods of tetrapropyl ammonium hydroxide (TPAOH) production via electrolysis, reaction of tetrapropyl ammonium halide with silver oxide, and ion-exchange suffer from high production costs, low quality, and environmental pollution. In this work, continuous bipolar membrane electrodialysis (BMED) is employed for the preparation of TPAOH from its halide as a sustainable alternative process. Novel ion-exchange membranes were developed for lab and pilot scale experiments, which indicate an acceptable current efficiency and energy consumption. The results indicate that a cell configuration with four compartments yielded the best results when the salt concentration was 0.3 mol L−1 and the current density was 200 A m−2. The highest conversion in electrodialysis was 91.6%, with a high purity of trace alkali metal ions and low Br− content (176 ppm) at a TPAOH concentration of 25%. The energy consumption is 1.897 kW h kg−1. Continuous pilot experiments demonstrate the feasibility of manufacturing TPAOH by direct splitting its halide for industrial application." @default.
• W2019166918 created "2016-06-24" @default.
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• W2019166918 date "2013-03-01" @default.
• W2019166918 modified "2023-10-16" @default.
• W2019166918 title "Preparation of highly pure tetrapropyl ammonium hydroxide using continuous bipolar membrane electrodialysis" @default.
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• W2019166918 doi "https://doi.org/10.1016/j.cej.2013.01.040" @default.
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