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- W2019169039 abstract "Poly[(methylsilyleneethynylenephenyleneethynylene)s-co-decamethylpentasiloxane] was synthesized by polycondensation reaction of di-Grignard reagent of diethynylbenzene with 1,9-dichlorodecamethylpentasiloxane and dichloromethylsilane. The copolymer is a liquid and soluble in common organic solvent at room temperature. The copolymer was characterized by FTIR, 1H-NMR, rheological analysis, and differential scanning calorimetry. The results show that the copolymer exhibits good processability and cures at about 170°C. The copolymer can be thermally cured to produce highly crosslinked copolymer. The thermal stability of the cured copolymer was measured by thermogravimetric analysis. The degradation temperature at 5% weight loss is 591°C and the residue yield at 1000°C is 86% in N2. Black, hard, and glassy ceramic was produced when the cured copolymer was heated above 1450°C under argon. The ceramic has high thermooxidative stability." @default.
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- W2019169039 date "2010-06-30" @default.
- W2019169039 modified "2023-10-16" @default.
- W2019169039 title "Synthesis and Characterization of Poly[(methylsilyleneethynylenephenyleneethynylene)s-<i>co</i>-decamethylpentasiloxane]" @default.
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- W2019169039 doi "https://doi.org/10.1080/10601325.2010.492274" @default.
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