Matches in SemOpenAlex for { <https://semopenalex.org/work/W2019401443> ?p ?o ?g. }
Showing items 1 to 80 of
80
with 100 items per page.
- W2019401443 endingPage "45" @default.
- W2019401443 startingPage "35" @default.
- W2019401443 abstract "Abstract In a search for means of preparing stable crystalline esters of sulfinic acids, yields from p-toluenesulfinic acid as a model were 53–92% with 1.1′-carbonyldiimidazole (CDI,2) as a coupling reagent for a variety of alcohols. The best coupling reagents were CDI and chlorotrimethylsilane (16). The agent 16 could be used with sulfinate salts, as could CDI with in situ acidification. The best alcohols were 1-adamantanol and p-nitrobenzyl alcohol. Among alkanesulfinic esters, methanesulfinates were unstable oils obtainable only in low yields, but 1-butanesulfinates were obtained in 52–5670 yield (although still as oils). As a stable disulfinic acid, 1,4-butanedisulfinic acid gave a nicely crystalline di-1-adamantyl ester (mp 123–125″C), but another alkanedisulfinate salt or acid that contained a disulfide moiety gave no diester by use either of 2 or 16." @default.
- W2019401443 created "2016-06-24" @default.
- W2019401443 creator A5006446539 @default.
- W2019401443 creator A5018769247 @default.
- W2019401443 date "1989-09-01" @default.
- W2019401443 modified "2023-09-24" @default.
- W2019401443 title "SULFINIC ACIDS AND RELATED COMPOUNDS. 21. PREPARATION OF CRYSTALLINE SULFINIC ESTERS1,2" @default.
- W2019401443 cites W1483329308 @default.
- W2019401443 cites W1516955863 @default.
- W2019401443 cites W1966580031 @default.
- W2019401443 cites W1970841968 @default.
- W2019401443 cites W2013813317 @default.
- W2019401443 cites W2019284494 @default.
- W2019401443 cites W2022145171 @default.
- W2019401443 cites W2046889012 @default.
- W2019401443 cites W2048136229 @default.
- W2019401443 cites W2055943066 @default.
- W2019401443 cites W2072750359 @default.
- W2019401443 cites W2149270926 @default.
- W2019401443 cites W2313776916 @default.
- W2019401443 cites W2322993630 @default.
- W2019401443 cites W2325111352 @default.
- W2019401443 cites W2343033922 @default.
- W2019401443 cites W2950227221 @default.
- W2019401443 cites W2952983826 @default.
- W2019401443 doi "https://doi.org/10.1080/10426508908046074" @default.
- W2019401443 hasPublicationYear "1989" @default.
- W2019401443 type Work @default.
- W2019401443 sameAs 2019401443 @default.
- W2019401443 citedByCount "5" @default.
- W2019401443 crossrefType "journal-article" @default.
- W2019401443 hasAuthorship W2019401443A5006446539 @default.
- W2019401443 hasAuthorship W2019401443A5018769247 @default.
- W2019401443 hasConcept C134121241 @default.
- W2019401443 hasConcept C178790620 @default.
- W2019401443 hasConcept C185592680 @default.
- W2019401443 hasConcept C191897082 @default.
- W2019401443 hasConcept C192562407 @default.
- W2019401443 hasConcept C27256138 @default.
- W2019401443 hasConcept C2776371256 @default.
- W2019401443 hasConcept C2776568683 @default.
- W2019401443 hasConcept C2780731314 @default.
- W2019401443 hasConcept C2781066024 @default.
- W2019401443 hasConcept C40875361 @default.
- W2019401443 hasConcept C518881349 @default.
- W2019401443 hasConcept C55493867 @default.
- W2019401443 hasConceptScore W2019401443C134121241 @default.
- W2019401443 hasConceptScore W2019401443C178790620 @default.
- W2019401443 hasConceptScore W2019401443C185592680 @default.
- W2019401443 hasConceptScore W2019401443C191897082 @default.
- W2019401443 hasConceptScore W2019401443C192562407 @default.
- W2019401443 hasConceptScore W2019401443C27256138 @default.
- W2019401443 hasConceptScore W2019401443C2776371256 @default.
- W2019401443 hasConceptScore W2019401443C2776568683 @default.
- W2019401443 hasConceptScore W2019401443C2780731314 @default.
- W2019401443 hasConceptScore W2019401443C2781066024 @default.
- W2019401443 hasConceptScore W2019401443C40875361 @default.
- W2019401443 hasConceptScore W2019401443C518881349 @default.
- W2019401443 hasConceptScore W2019401443C55493867 @default.
- W2019401443 hasIssue "1-2" @default.
- W2019401443 hasLocation W20194014431 @default.
- W2019401443 hasOpenAccess W2019401443 @default.
- W2019401443 hasPrimaryLocation W20194014431 @default.
- W2019401443 hasRelatedWork W1963589499 @default.
- W2019401443 hasRelatedWork W1991750636 @default.
- W2019401443 hasRelatedWork W2047888616 @default.
- W2019401443 hasRelatedWork W2048915055 @default.
- W2019401443 hasRelatedWork W2093796341 @default.
- W2019401443 hasRelatedWork W2096882331 @default.
- W2019401443 hasRelatedWork W2147427301 @default.
- W2019401443 hasRelatedWork W2326148101 @default.
- W2019401443 hasRelatedWork W2949184651 @default.
- W2019401443 hasRelatedWork W2953155228 @default.
- W2019401443 hasVolume "45" @default.
- W2019401443 isParatext "false" @default.
- W2019401443 isRetracted "false" @default.
- W2019401443 magId "2019401443" @default.
- W2019401443 workType "article" @default.