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- W2019468960 abstract "A new voltammetric method was developed for simultaneous determination of amlodipine (AML) and valsartan (VAL) in synthetic urine and combined pharmaceutical formulations. The anodic peak potentials of AML and VAL oxidation at a cathodically pretreated boron-doped diamond electrode were found to be 0.791 V and 1.37 V (vs. Ag/AgCl (3.0 mol L−1 KCl)), respectively, by cyclic voltammetry, in Britton–Robinson buffer solution (pH 5.0). Using square-wave voltammetry, the obtained analytical curves were linear in the AML and VAL concentration range from 0.497–28.0 μmol L−1 and 19.8–280 μmol L−1 with detection limits of 0.0764 μmol L−1 and 0.193 μmol L−1, respectively. The proposed method was successfully applied in the simultaneous determination of AML and VAL in various combined dosage forms available in the market, with results similar to those obtained using a comparative chromatography method. Additionally, adequate recovery results were obtained for the simultaneous determination of AML and VAL in synthetic urine sample. Due to its adequate linearity, the proposed method could be a good alternative for simultaneous determination of AML and VAL in all the different dosages available in the market, even in synthetic urine sample." @default.
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- W2019468960 date "2015-02-01" @default.
- W2019468960 modified "2023-09-23" @default.
- W2019468960 title "Electroanalytical application of a boron-doped diamond electrode: Improving the simultaneous voltammetric determination of amlodipine and valsartan in urine and combined dosage forms" @default.
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- W2019468960 doi "https://doi.org/10.1016/j.jelechem.2014.11.034" @default.
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