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• W2019470830 abstract "We report on a one-pot, highly selective chemistry to remove residual catalysts from single-walled carbon nanotubes (SWNTs). The impurities, initially present at approximately 35 wt % and mostly as carbon-coated iron nanoparticles, can be driven below 5 wt % with nearly no loss of SWNTs. The carbon-coated iron impurities are dissolved simply by reacting with an aqueous mixture of H2O2 and HCl at 40-70 degrees C for 4-8 h. This purification combines two known reactions involving H2O2 and HCl, respectively; however, by combining these two typically inefficient reactions into a one-pot reaction, the new process is surprisingly selective toward the removal of the metal impurities. This high selectivity derives from the proximity effect of the iron-catalyzed Fenton chemistry. At pH approximately 1-3, iron is dissolved upon exposure, avoiding the otherwise aggressive iron-catalyzed digestion of SWNTs by H2O2. This extremely simple and selective chemistry offers a green and scalable process to purify carbon nanotube materials." @default.
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• W2019470830 date "2007-01-24" @default.
• W2019470830 modified "2023-10-07" @default.
• W2019470830 title "A Highly Selective, One-Pot Purification Method for Single-Walled Carbon Nanotubes" @default.
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• W2019470830 doi "https://doi.org/10.1021/jp068229+" @default.
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