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• W2019480972 endingPage "353" @default.
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• W2019480972 abstract "This report presents detailed studies on the elemental analysis, vibrational spectroscopy, thermal stability and electrical spectroscopy of two new hybrid inorganic–organic polymers which have been synthesised by a sol–gel method using glycerol and zirconium(IV)butoxide as precursors. These materials have been doped by means of 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide (EMIm-TFSI) ionic liquid (IL), which is insoluble in water. The elemental composition of the obtained polymers [Zr(C6O5H11)] (1) and [Zr(C11O4H31)] (2) has been determined by CHN analysis and by ICP-AES measurements. FT-IR and FT-Raman spectroscopy investigations have been performed to study the molecular structure of the polymers and the interactions of EMIm-TFSI with the host networks. Differential scanning calorimetry measurements show the presence of at least one glass transition temperature (Tg) in both 1 and 2 materials. The broadband dielectric spectroscopic measurements have been carried out between 10−2 Hz to 10 MHz from −100 °C to 100 °C with a 5 °C step. The conductivities of the polymers 1 and 2 have been found to be in the order of 10−8 to 10−11 S cm−1 at 25 °C, so they can be defined as dielectric materials. After doping 2 with EMIm-TFSI, the conductivity at 25 °C of the obtained complex [Zr(C11O4H31)]15/(EMIm-TFSI) (2′) increased three orders of magnitude resulting ca. 10−5 S cm−1. The permittivity spectra revealed two relaxation bands which were attributed to the α relaxation modes of the polymer networks." @default.
• W2019480972 created "2016-06-24" @default.
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• W2019480972 date "2010-01-01" @default.
• W2019480972 modified "2023-10-18" @default.
• W2019480972 title "New hybrid inorganic–organic polymer electrolytes based on Zr(O(CH2)3CH3)4, glycerol and EMIm-TFSI ionic liquid" @default.
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• W2019480972 doi "https://doi.org/10.1016/j.jpowsour.2009.06.088" @default.
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