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- W2019504369 abstract "A polymer-bound cation system of the triphenylmethyl type has been synthesized via a method in which the first step is lithiation of polystyrene. The final step in the synthesis of the polystyrene-bound triphenylmethyl carbocation system was either conversion of the corresponding polymer-bound triphenylmethyl chloride with AlCl3 or the conversion of the polymer-bound triphenylmethyl alcohol with perchloric acid. The various functionalized polymer samples were characterized by solid-state 13C NMR, which showed that, for the polymer-bound triphenylmethyl alcohol system, there are 0.59 mmol of carbinol moieties per gram of polymer. The polymer-bound carbocation system was found to be surprisingly stable, even to moisture in air, and can readily be regenerated from its hydrolysis product. The polymer-bound carbocation system is effective as a catalyst in a Michael addition reaction and as a hydride acceptor reagent in a Dauben-type hydride transfer reaction." @default.
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- W2019504369 date "1997-12-01" @default.
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- W2019504369 title "Synthesis and Solid-State 13C NMR Study of Polymer-Bound Triphenylmethyl Cations" @default.
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- W2019504369 doi "https://doi.org/10.1021/ma9710040" @default.
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