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• W2019854908 startingPage "2999" @default.
• W2019854908 abstract "Divalent organolead compounds (plumbylenes; Tip2Pb (6; Tip = 2,4,6-triisopropylphenyl) and Tbt(R)Pb (7a, R = Tbt; 7b, R = Ttm; 7c, R = Tip; 7d, R = Dis; Tbt = 2,4,6-tris[bis(trimethylsilyl)methyl]phenyl, Ttm = 2,4,6-tris[(trimethylsilyl)methyl]phenyl, and Dis = bis(trimethylsilyl)methyl)) were synthesized by taking advantage of kinetic stabilization afforded by bulky substituents and characterized by UV/vis and 207Pb NMR spectroscopy. X-ray structural analysis revealed that plumbylene 7a has a V-shaped, monomeric structure. Reactions of these plumbylenes with methyl iodide, carbon tetrabromide, diphenyl disulfide, diphenyl diselenide, and elemental sulfur are described. New methods for the synthesis of plumbylenes from tetravalent organolead compounds, by reductive debromination of dibromoplumbanes and exhaustive desulfurization of tetrathiaplumbolanes, were developed." @default.
• W2019854908 created "2016-06-24" @default.
• W2019854908 creator A5038178281 @default.
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• W2019854908 date "1999-07-07" @default.
• W2019854908 modified "2023-10-14" @default.
• W2019854908 title "Synthesis, Structure, and Reactivity of Kinetically Stabilized Divalent Organolead Compounds (Plumbylenes)" @default.
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• W2019854908 doi "https://doi.org/10.1021/om990188z" @default.
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