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- W2019908532 abstract "Die Synthese des Aporphinalkaloids (R,S)-Bulbocapnin (1a) wird beschrieben. Schlüsselschritt zweier hier verfolgter Reaktionswege ist die nichtoxidative Photocyclisierung eines halogenierten 1-Benzyl-tetrahydroisochinolins 12 bzw. des Stilbenderivates 14. Während der Weg, ausgehend von 12, erwartungsgemäß zu (R,S)-Bulbocapnin führte, gelangte man über das Stilben 14 überraschend zu dem Bulbocapnin Isomeren (R,S)-Cassythicin (1b). Experiments on photochemical synthesis of Bulbocapnin The synthesis of the aporphin alkaloid (R,S)-bulbocapnine (1a) is described. The keystep of both reaction paths is the non-oxidative photocyclization of a halogenated 1-benzyl-tetrahydroisoquinoline 12 and that of the stilbene derivative 14. Whereas the route starting from 12 led to (R,S)-bulbocapnine, as expected, the stilbene surprisingly led to the bulbocapnine isomer (R,S)-cassythicine (1b)." @default.
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- W2019908532 date "1988-01-01" @default.
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- W2019908532 title "Versuche zur photochemischen Synthese von Bulbocapnin" @default.
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- W2019908532 doi "https://doi.org/10.1002/ardp.19883210308" @default.
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