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- W2019910226 abstract "Abstract The synthesis of simple single source molecular precursor based on metal alkoxides of the type,[(MMPEP)Al(μ-OBnCH 2 Cl)] 2 ( 1 ),[(MMPEP-H)Li·(BnOH)] 2 ( 2 ) and[(MMPEP-H)Li·(HOB- n CH 2 Cl)] 2 ( 3 ) has been reported herein. Complex 1 was prepared by the reaction of[(MMPEP)Al(CH 3 )(Et 2 O)] with p -(chloromethyl)benzyl alcohol. The reaction of 2,2′-methylene-bis(4,6-di(1-methyl-1-phenylethyl)phenol) (MMPEP-H 2 ) with n BuLi, BnOH or p -(chloromethyl)benzyl alcohol was added to give complexes 2 and 3 , respectively. Among them, only complex 1 shows excellent catalytic properties towards ring-opening polymerization (ROP) of e-caprolactone. However, complexes 2 and 3 are active for ROP of l -lactide only. Block copolymers of poly(e-caprolactone)-β-polyacrylonitrile and poly( l -lactide)-β-polyacrylonitrile were synthesized by using a technique known as atom transfer radical polymerization (ATRP) and the ring opening polymerization (ROP). TEM micrograph of PCL-β-PAN shows the microphase property with the help of self-assembly." @default.
- W2019910226 created "2016-06-24" @default.
- W2019910226 creator A5013410859 @default.
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- W2019910226 date "2014-04-01" @default.
- W2019910226 modified "2023-09-26" @default.
- W2019910226 title "Synthesis and characterization of alkoxy derivatives with double-headed initiators for the preparation of poly(ε-caprolactone)-β-polyacrylonitrile (PCL-β-PAN) and poly(l-lactide)-β-polyacrylonitrile (PLLA-β-PAN) copolymers" @default.
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- W2019910226 doi "https://doi.org/10.1016/j.arabjc.2010.10.026" @default.
- W2019910226 hasPublicationYear "2014" @default.
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