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• W2019912189 abstract "The first stable arsaallene, ArAsCCR2 1 (Ar = 2,4,6-tri-tert-butylphenyl, CR2 = fluorenylidene), has been synthesized by a one-pot procedure involving the successive addition of n-butyllithium and fluorenone to the new arsaalkene ArAsC(Br)SiMe3, which presents a Z configuration and a short AsC bond length (1.789(3) Å). An X-ray crystallographic structure determination of air and thermally stable 1 proves its allenic geometry (AsC(1)C(2) bond angle 169.72(19)°, angle between the fluorenylidene plane and the C(15)AsC(1)C(2) mean plane 79.3°) with very short AsC(1) and C(1)C(2) double-bond lengths (1.754(2) and 1.314(3) Å)." @default.
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• W2019912189 date "2002-03-21" @default.
• W2019912189 modified "2023-09-25" @default.
• W2019912189 title "From the New Arsaalkene ArAsC(Br)SiMe₃ to the First Stable Arsaallene, ArAsCCR₂ (Ar = 2,4,6-Tri-<i>tert</i>-butylphenyl, CR₂ = Fluorenylidene)" @default.
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• W2019912189 doi "https://doi.org/10.1021/om011075u" @default.
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