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- W2019912549 abstract "Abstract X-ray photoelectron spectroscopy (XPS) was used to determine Fe(III)/ΣFe in individual biotite crystals in thin sections of ten metapelites and one syenite. The in situ XPS analyses of Fe(III)/∑Fe in biotite crystals in the metapelites were compared with published Fe(III)/IFe values determined by Mossbauer spectroscopy (MS) for mineral separates from the same hand samples. The difference between Fe(HI)/ΣFe by the two techniques was greatest for samples with the lowest Fe(III)/ΣFe (by MS). For eight metamorphic biotites with Fe(III)/ΣFe = 9–27% comparison of the two techniques yielded a linear correlation of r = 0.94 and a statistically acceptable fit of [Fe(III)/ΣFe]xps = [Fe(IIl)/ ΣFe]ms. The difference between Fe(III)/1Fe by the two techniques was greater for two samples with Fe(III)/ΣFe ≤ 6% (by MS). For biotite in the syenite sample, Fe(III)/ΣFe determined by both in situ XPS and bulk wet chemistry/electron probe microanalysis were similar. This contribution demonstrates that XPS can be used to analyze bulk Fe(III)/ΣFe in minerals in thin sections when appropriate precautions are taken to avoid oxidation of the near-surface during preparation of samples." @default.
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- W2019912549 date "1997-11-01" @default.
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- W2019912549 title "Quantitative determination of the oxidation state of iron in biotite using X-ray photoelectron spectroscopy: II. In situ analyses" @default.
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- W2019912549 doi "https://doi.org/10.1016/s0016-7037(97)00264-0" @default.
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