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• W2019941278 abstract "The mixed gallium transition-metal complexes [FeCl[Ga(2)((t)Bu)(4)(neol)(2)]] (1) and [M[Ga(2)((t)Bu)(4)(neol)(2)]], M = Co (2), Ni (3), Cu (4), have been prepared by the reaction of [Ga(2)((t)Bu)(4)(neol-H)(2)] (neol-H(2) = 2,2-dimethyl-propane-1,3-diol) with the appropriate metal halide and Proton Sponge. Compounds 1-4 have been characterized by NMR (3), UV/vis, and IR spectroscopy and magnetic susceptibility (solution and solid state), and their molecular structures have been confirmed by X-ray crystallography. The molecular structure of compounds 1-4 consists of a tetracyclic core formed from two four-membered and two six-membered rings. The central metal atom adopts a square pyramidal (1) or square planar (2-4) geometry. The magnetic susceptibilities for 1, 2, and 4 are as expected for strong ligand field environments. On the basis of spectroscopic and structural data, the [Ga(2)((t)Bu)(4)(neol)(2)](2-) ligand appears to be more flexible than other chelating ligands; this is proposed to be due to the flexibility in the O-Ga-O bond angle." @default.
• W2019941278 created "2016-06-24" @default.
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• W2019941278 date "2002-01-17" @default.
• W2019941278 modified "2023-10-18" @default.
• W2019941278 title "Transition-Metal Complexes of a Bifunctional Tetradentate Gallium Alkoxide Ligand" @default.
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• W2019941278 doi "https://doi.org/10.1021/ic0106773" @default.
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