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- W2019943301 abstract "Rotational Echo DOuble Resonance (REDOR) NMR is an oft-demonstrated tool for measuring distance between isolated IS spin pairs. Its application to more complex ISn spin networks (n>1), however, is rare, as in these systems the interpretation of the results is model-dependent–while it is precisely the measurement of multiple distances which is required for molecular structure elucidation. Recently, Θ-REDOR was introduced and was shown to improve interpretability at the cost of signal intensity. In this paper we analyze generalizations to the REDOR pulse sequence, and present a new experimental procedure which allows for simultaneous distance determinations in larger spin systems with improved signal intensity. Experimental data are presented for the IS2 spin system glycine-C213-N15." @default.
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- W2019943301 date "2000-07-15" @default.
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- W2019943301 title "Multiple simultaneous distance determinations: Application of rotational echo double resonance nuclear magnetic resonance to IS2 spin networks" @default.
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- W2019943301 doi "https://doi.org/10.1063/1.481887" @default.
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