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• W2019957679 abstract "Abstract A new method for the synthesis of Ce 0.80 Sm 0.20 O 1.90 is presented. A drying of a solution of ethylene glycol and stoichiometric amounts of the acetates Ce(C 2 H 3 O 2 ) 3 · x H 2 O and Sm(C 2 H 3 O 2 ) 3 · x H 2 O resulted in a highly crystalline product of [Ce 0.80 Sm 0.20 (C 2 H 3 O 2 ) 3 (C 2 H 6 O 2 )] n , a new chained polymeric coordination compound. With the calcination of this precursor at 900 °C and sintering at 1150 °C, pure Ce 0.80 Sm 0.20 O 1.90 , was obtained with the desired homogeneity and density. This paper reports elemental (CHN and ICP-MS) and single crystal X-ray structure analyses of the precursor [Ce 0.80 Sm 0.20 (C 2 H 3 O 2 ) 3 (C 2 H 6 O 2 )] n . Its thermal decomposition to Ce 0.80 Sm 0.20 O 1.90 has been studied via HT-XRD and TG–DTA analysis. The structure and composition of Ce 0.80 Sm 0.20 O 1.90 was also confirmed by powder XRD (Rietveld refinement)." @default.
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• W2019957679 date "2012-08-01" @default.
• W2019957679 modified "2023-10-18" @default.
• W2019957679 title "A new simple synthesis and characterization of Sm-doped ceria and its homogeneous precursor [Ce0.80Sm0.20(Ac)3(Gly)]n" @default.
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• W2019957679 doi "https://doi.org/10.1016/j.jeurceramsoc.2012.02.008" @default.
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