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- W2019994656 abstract "We describe the synthesis of 2′-[18F]fluoroflumazenil (FFMZ), which differs from the typically used [18F]fluoroethylflumazenil (FEFMZ) for benzodiazepine receptor imaging. For one-pot one-step labeling, the precursors, 2′-tosyloxyflumazenil (TFMZ) and 2′-mesyloxyflumazenil (MFMZ), were synthesized in three steps. The precursors were successfully labeled with no-carrier-added 18F-fluoride which was activated by repeated azeotropic distillation with Kryptofix 2.2.2./potassium carbonate in MeCN. An automated system for labeling and purification of [18F]FFMZ was developed. Labeling efficiency and radiochemical purity of [18F]FFMZ after synthesis by the automated system were 68% and 98%, respectively. Specific binding of [18F]FFMZ to central benzodiazepine receptor of rats was demonstrated by phosphoimaging." @default.
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- W2019994656 date "2003-05-01" @default.
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- W2019994656 title "Novel one-pot one-step synthesis of 2′-[18F]fluoroflumazenil (FFMZ) for benzodiazepine receptor imaging" @default.
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- W2019994656 doi "https://doi.org/10.1016/s0969-8051(03)00030-1" @default.
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