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• W2020008518 startingPage "1786" @default.
• W2020008518 abstract "The gold-catalyzed conversion of allyl-(ortho-alkynylphenyl)methyl ethers was investigated, and allylated isochromenes were obtained. An optimization of the catalysis conditions with respect to different phosphane and carbene ligands on gold, different counterions, and different solvents was conducted. Subsequently, the scope and limitations of this reaction were investigated with 21 substrates. The mechanistic studies show an allylic inversion, as supported by NMR data and an X-ray crystal structure analysis, as well as an intermolecular reaction, as determined by crossover experiments. There is no competition of protodeauration even in the presence of water. All these observations differ from other related conversions and clearly indicate product formation by a [3,3]sigmatropic rearrangement in the step forming the new CC bond." @default.
• W2020008518 created "2016-06-24" @default.
• W2020008518 creator A5007635998 @default.
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• W2020008518 creator A5084670164 @default.
• W2020008518 date "2013-05-31" @default.
• W2020008518 modified "2023-10-17" @default.
• W2020008518 title "[3,3]-Sigmatropic Rearrangement Step in the Gold-Catalyzed Cyclization of Allyl-(<i>ortho</i>-alkinylphenyl)methyl Ethers" @default.
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• W2020008518 doi "https://doi.org/10.1002/asia.201300324" @default.
• W2020008518 hasPubMedId "https://pubmed.ncbi.nlm.nih.gov/23729410" @default.
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