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- W2020031567 abstract "The advent of the sol–gel technique over the past several decades and the recognition of its excellent flexibility for synthesizing a large variety of oxide ceramics and glasses in both bulk and thin-film forms has generated considerable interest in using solution-based processes to prepare ceramic materials. Because of the success of the sol–gel technique, a number of other chemical processes have been developed utilizing metalorganic/organometallic starting materials to create molecularly architectured precursors, which have proven effective in synthesizing both oxide and non-oxide materials. In the present study, two different chemical approaches have been implemented to synthesize non-oxides (sulfides and nitrides) of reactive transition-metal elements. Accordingly, a novel thio-sol–gel process for preparing TiS2 and NbS2 powders has been studied. In the case of TiS2 synthesis, the chemical reaction has been examined in detail using Fourier-transform infrared spectroscopy (FTIR) and gas chromatography (GC). The effects of modification of the titanium precursor on the morphology of the final sulfide have also been investigated and are discussed. A second, more generalized process has been developed for synthesizing homogeneous precursors in multicomponent systems. Its utilization in preparing ternary nitrides has been demonstrated, and is also presented. © 1997 by John Wiley & Sons, Ltd." @default.
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- W2020031567 date "1997-02-01" @default.
- W2020031567 modified "2023-09-23" @default.
- W2020031567 title "Low-Temperature Chemical Approaches for Synthesizing Sulfides and Nitrides of Reactive Transition Metals" @default.
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- W2020031567 doi "https://doi.org/10.1002/(sici)1099-0739(199702)11:2<163::aid-aoc564>3.0.co;2-s" @default.
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