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- W2020046956 abstract "Measurements of the 59Co quadrupole parameters in a single crystal of Co(NH3)6Cl3 over the temperature range 404 > T > 93 K are reported. Above 330 K three non-equivalent Co(NH3)63+ octahedra execute fast isotropic reorientations while the fourth octahedron is stationary. Fair agreement between experimental parameters and those obtained from an electric field gradient calculation in which each electric charge is placed at its time-averaged position, is obtained. The anomalous behavior of two of the coupling constants above 390 K is attributed to the decomposition of the material. As the temperature is lowered to about 300 K, the isotropic motions at two of the nonequivalent octahedra are reduced to uniaxial reorientations about two- or four-fold axes of the octahedra. At about 200 K these motions freeze and three of the nonequivalent octahedra are stationary. The reorientations at the other site freeze at about 100 K. A phase transition, accompanied by an increase of the number of 59Co NMR lines, is observed at about 170 K." @default.
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- W2020046956 date "1973-01-01" @default.
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- W2020046956 title "Phase transition and far i.r. spectrum of hexammine cobaltous chloride crystal" @default.
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- W2020046956 doi "https://doi.org/10.1016/0022-3697(73)90069-3" @default.
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