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• W2020089213 abstract "Abstract The 31 P chemical shift (CS) tensors of the 1,3,2‐diazaphospholenium cation 1 and the P ‐chloro‐1,3,2‐diazaphospholenes 2 and 3 and the 31 P and 19 F CS tensors of the P ‐fluoro‐1,3,2‐diazaphospholene 4 were characterized by solid‐state 31 P and 19 F NMR studies and quantum chemical model calculations. The computed orientation of the principal axes system of the 31 P and 19 F CS tensors in the P ‐fluoro compound was found to be in good agreement with experimentally derived values obtained from evaluation of P–F dipolar interactions. A comparison of the trends in the chemical shifts of 1 – 4 with further available literature data confirms that the unique high shielding of δ 11 in the cation 1 can be related to the effective π‐conjugation in the five‐membered heterocycle, and that a further systematic decrease in δ 11 for the P ‐halogen derivatives 2 – 4 is attributable to the increased perturbation of the π‐electron distribution by interaction with the halide donor. Copyright © 2002 John Wiley & Sons, Ltd." @default.
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• W2020089213 date "2002-07-23" @default.
• W2020089213 modified "2023-10-03" @default.
• W2020089213 title "The bonding situation in 1,3,2-diazaphospholene derivatives as studied by solid-state NMR spectroscopy" @default.
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• W2020089213 doi "https://doi.org/10.1002/mrc.1065" @default.
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