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- W2020101641 abstract "Substitution of phenyl groups in Ph2SbR (1) (R=Me3SiCH2) with chlorine atoms leads to RSbCl2 (2). Reduction of 2 with magnesium in tetrahydrofuran gives red crystals of (RSb)n (3) and a black solid containing the polymer (RSb)x. Solutions of 3 in C6D6 are yellow. They consist of an equilibrium mixture of (RSb)5 and (RSb)4. The reaction between 2 and cobaltocene in tetrahydrofuran or C6D6 leads to the polymer (RSb)x and to the salt [COCp2]+[RSbCl3]− (4). The structure of 4 has been determined by single-crystal X-ray diffraction. It contains a centrosymmetric double-chlorine-bridged dimeric anion. The ditellurostibane RSb(Te-p-Tol)2 (5) has been obtained with a quantitative yield through a complete reaction between 3 and (p-TolTe)22. Compound 5 has been detected in the product mixtures resulting from reactions of polymeric (RSb)x with (p-TolTe)2 or by reducing p-TolTeCl3 and RSbCl2 with magnesium in tetrahydrofuran." @default.
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- W2020101641 date "1995-10-01" @default.
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- W2020101641 title "Synthesis of (Me3SiCH2Sb)n and reactions with ditellurides: crystal structure of [Cp2Co][Me3SiCH2SbCl3]" @default.
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- W2020101641 doi "https://doi.org/10.1016/0022-328x(95)05621-u" @default.
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