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- W2020114718 abstract "An analytical method for the determination of glyphosate and its principal metabolite, aminomethylphosphonic acid (AMPA), in water of different hardnesses (5, 20, and 30 °DH, french hardness) has been developed. Samples were fortified at different levels (0.05, 0.1, 1, and 5 μg/L) and were purified by column chromatography on ion-exchange resins. After derivatization with TFAA/HFB mixture, the derivatives were quantified by using capillary gas chromatography with an ion-trap tandem mass spectrometric detector. Analytical conditions for MS/MS detection were optimized, and the quantification was carried out on the sum of areas of the three most representative ions: m/z 283, 223, and 181 for AMPA and m/z 440, 321, and 261 for glyphosate. The limit of quantification was demonstrated to be at 0.05 μg/L for each compound. The mean recovery value and the relative standard deviation (n = 65) were 93 and 12% for AMPA and 95 and 13% for glyphosate." @default.
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- W2020114718 date "2000-07-11" @default.
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- W2020114718 title "Determination of Glyphosate and Aminomethylphosphonic Acid Residues in Water by Gas Chromatography with Tandem Mass Spectrometry after Exchange Ion Resin Purification and Derivatization. Application on Vegetable Matrixes" @default.
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- W2020114718 doi "https://doi.org/10.1021/ac000041d" @default.
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