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- W2020116023 abstract "Abstract Reaction of VCl3 with 2-mercapto-3-pyridinol (H2mpp) in the presence of CH3ONa yields (VO(Hmpp)2 · CH3CN (1). The coordination geometry around the vanadium is square pyramidal, with a VO double bond of 1.602(6) A and average VS and VO distances of 2.392 and 1.943 A, respectively. The mpp ligands behave as the thione tautomer with the N atoms prontonated rather than the thiol alternative form. The intermolecular hydrogen bonding interactions between the protonated N atoms and the terminal O or the coordinated O atoms of mpp ligands result in an infinite two-dimensional network of VO(Hmpp)2. Complex (1) has been characterized by infrared, and EPR spectroscopic studies." @default.
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- W2020116023 date "1998-01-01" @default.
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- W2020116023 title "A novel network of bis(2-mercapto-3-pyridinol)oxovanadium(IV)_ based on hydrogenbond interactions: synthesis, structure and EPR spectroscopic properties" @default.
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- W2020116023 doi "https://doi.org/10.1016/s0277-5387(97)00295-7" @default.
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